Equipment and Calibration

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Equipment Entry

Instrument:Gas Analyzer
Manufacture:Licor
Model No:LI-7700
Serial No:TG1-0155
Tag No:
Acquisition Date:2010-12-15
Project:NSF-Methane
Location on 2024-01-11:Hill Slough,
Notes: Arrived with LI7550 sn AIU-397. Dead on arrival returned for repair. IPV6 = fe80:0000:021c:94ff:fe04:04fe
IPV4 = 169.254.125.82

Documents

Manual: Collecting_LI-7700_Ethernet_Data.pdf
Manual: LI-7700_Manual_V2_201103.pdf
Manual: LI-7700_Manual_V3_201312.pdf

History

Rec No.DateLoc FromTitleLoc ToNotes
6807 2024-08-07 Hill Slough Calibration Hill Slough Calibration Location: Hill Slough
Last calibration: 2024-01-10
RSSI=81%, Optical RH=4%
Ambient P=101.1kPa, Tair=27.2C
Zero Air at 1750psi, AMP CA03923 3.3865 at 1900
CH4 Zero Offset: .005ppm
CH4 Span Offset: 0.0235ppm
Notes: Breezy, not too windy for once. Try to come first thing in the morning to avoid afternoon winds.
6530 2024-01-11 Lab none Installed Hill Slough Gas Analyzer CH4 Installed at HS to replace sn TG1-0421, which was removed for calibration
6523 2024-01-10 Lab Calibration Lab Calibration Location: Lab
Last calibration: 2023-06-15
RSSI=91%, Optical RH=21%
Ambient P=100.46kPa, Tair=21.3C
Zero Air at 500psi, AMP CA04119 4.2238 at 750
CH4 Zero Offset: -.03ppm
CH4 Span Offset: -.0188ppm
Notes: This sensor was removed from WP with its decommissioning. Back in the lab, it had revert to default heater settings and its clock was off (laptop=11:46, 7700=18:51, "Etc/GMT+8" on slave). I changed the clock setting to automatic, set the clock to match the laptop time, changed the clock setting back to slave, and then rebooted. The time was correct after reboot but we should double-check it after conencting to the 7550 in the field. I changed the heater settings back to our usual. Before calibration, I flushed the optics headspace down to 10% and swapped in a bottle of fresh drierite.
6519 2024-01-04 West Pond Gas Analyzer CH4 Removed Lab none Removed from WP tower with initial decommissioning of the site
6303 2023-06-15 West Pond Calibration West Pond Calibration Location: West Pond
Last calibration: 2023-01-18
RSSI=89%, Optical RH=13%
Ambient P=101.0kPa, Tair=26.2C
Zero Air at 1100psi, AMP CA04119 4.2238 at 1050
CH4 Zero Offset: 0ppm
CH4 Span Offset: -.0088ppm
Notes: Zero was right on! Since the optics RH=13% which is pretty good, we did not flush its headspace or change its desiccant. The heater and cleaning settings were set to the default (maybe because of recent power outages). I updated both to what I remember to be our usual settings.
6167 2023-01-18 West Pond Calibration West Pond Calibration Location: West Pond
Last calibration: 2022-06-09
RSSI=81%, Optical RH=10%
Ambient P=101.9kPa, Tair=12.3C
Zero Air at 1500psi, AMP CA04396 1.9317 at 1125
CH4 Zero Offset: .008ppm
CH4 Span Offset: .0103ppm
Notes: Since optics RH = 10%, I did not change desiccant or flush headspace after calibration.
5899 2022-06-09 West Pond Calibration West Pond Calibration Location: West Pond
Last calibration: 2021-12-06
RSSI=90%, Optical RH=3%
Ambient P=101.1kPa, Tair=30.1C
Zero Air at 400psi, AMP CA04119 4.2238 at 1550
CH4 Zero Offset: .016ppm
CH4 Span Offset: .0028ppm
Notes: Hot but relatively still at this site
5807 2022-04-20 Lab none Installed West Pond Gas Analyzer CH4 Installed at WP to replace TG1-0421, which was removed last week for power issues.
5795 2022-04-13 Bouldin Alfalfa Gas Analyzer CH4 Removed Lab none Removed from Bouldin Alfalfa and brought back to the lab because we will use it to replace the faulty one from WP. I removed the power cable as well since the WP power cable could be bad. The wash power, wash tubing, and Ethernet cable are still there.
5610 2021-12-01 Bouldin Alfalfa Calibration Bouldin Alfalfa Calibration Location: Bouldin Alfalfa
Last calibration: 2021-05-10
RSSI=84%, Optical RH=3%
Ambient P=101.7kPa, Tair=21.4C
Zero Air at 1050psi, AMP CA04396 1.9317 at 1700
CH4 Zero Offset: .022ppm
CH4 Span Offset: -.0087ppm
Notes: Relatively still day. Zero air tank pressure uncertain--wonky regulator.
5247 2021-04-15 Lab none Installed Bouldin Alfalfa Gas Analyzer CH4 Installed on the BA tower after factory repair/calibration.
5238 2021-04-14 Factory none Repair Lab none The following were replaced: spinning mirror motor and base plate assembly, spars, digital board (had water damage in area of RTC), pressure sensor (was totally soaked and corroded). Factory calibration on 2021-03-25.
5258 2021-03-25 Factory none Calibration Factory none Factory calibration with repair of the instrument. New Coefficients:
5104 2021-02-04 Lab none Shipped Factory none Shipped to Licor and RMA 00225226 for evaluation after being submerged when the BC tower fell in the storm last week.
5103 2021-02-01 Lab none Tested Lab none On the 29th I removed this sensor from being submerged after the BC tower fell just after midnight on the morning of the 27th. On the evening of the 29th, about 1/2 cup of water came out of the bottom when I removed the base. I removed the desiccant bottle in the head and saw no evidence that water had leaked in there. I left dry air flowing inside the base over night. On the 30th I removed the bottom case and only saw minor water damage on the pressure sensor. On the 1st, after consultation with Licor, I powered up the analyzer and got green power and status lights but no communications on the Ethernet. It will need to be returned to Licor for further evaluation.
5070 2021-01-29 Bouldin Corn Gas Analyzer CH4 Removed Lab none Removed due to the tower falling over in the storm near midnight on 2021-01-26/27. Completely submerged
4983 2020-11-20 Bouldin Corn Gas Analyzer CH4 Calibration Bouldin Corn Gas Analyzer CH4 Calibration Location: Bouldin Corn
Last calibration: 2020-05-19
RSSI=88%, Optical RH=20%
Ambient P=102.5kPa, Tair=9.4C
Zero Air at 575psi, AMP CA3923 3.121 at 550
CH4 Zero Offset: 0ppm
CH4 Span Offset: 0.009ppm
Notes: Foggy day with a litle breeze. The RSSI after cleaning was 50, but jumped up to 88 after putting hood on and running dry air through.
4455 2020-05-19 Bouldin Corn Calibration Bouldin Corn Calibration Location: Bouldin Corn
Last calibration: 2019-12-04
RSSI=88%, Optical RH=9%
Ambient P=101.6kPa, Tair=17.5C
Zero Air at 900psi, AMP CA3923 3.121 at 1000
CH4 Zero Offset: 0.022ppm
CH4 Span Offset: -0.001ppm
Notes: Seems stable (2nd calibration after sensor fell off BC tower). Breezy day.
4303 2019-12-13 Lab none Installed Bouldin Corn Gas Analyzer CH4 Re-installed at Bouldin Corn after re-assembling tower.
4307 2019-12-11 Lab none Maintenance Lab none Joe painted on white outdoor-furniture paint on the spar with cracked paint. We ran the sensor for 2 days in the lab connected to the lab 7550, and the data seemed ok, so it seems ready to deploy in the field again.
4230 2019-12-04 Lab none Calibration Lab none Calibration Location: Lab
Last calibration: 2019-10-22
RSSI=87%, Optical RH=7%
Ambient P=99.9kPa, Tair=20.2C
Zero Air at 900psi, AMP CA4396 1.9497 at 650
CH4 Zero Offset: -0.091ppm
CH4 Span Offset: 0.011ppm
Notes: Testing this sensor after it fell down with the BC tower. First calibration. Offsets seem reasonable. May be a little less stable , or I was just impatient waiting for the span gas to equilibrate.
4270 2019-12-02 Bouldin Corn Gas Analyzer CH4 Removed Lab none Removed from Bouldin Corn site and brought back to the lab after the tower fell down during a rain/wind storm on 2019-11-26.
4113 2019-10-22 Bouldin Corn Gas Analyzer CH4 Calibration Bouldin Corn Gas Analyzer CH4 Calibration Location: Bouldin Corn
Last calibration: 2019-04-11
RSSI=89.5%, Optical RH=26%
Ambient P=102.1kPa, Tair=17.2C
Zero Air at 1350psi, AMP CA03923 3.121 at 1400
CH4 Zero Offset: 0.024ppm
CH4 Span Offset: -0.005ppm
Notes: Light breeze, swapped optical desiccant after calibration using cal gas to dry head space. New RH 7%.
3938 2019-04-25 Bouldin Corn Gas Analyzer CH4 Upgrade Bouldin Corn Gas Analyzer CH4 The LI-7700 firmware was upgraded from v1.0.21 to v1.0.27 mostly minor bug fixes see change log https://www.licor.com/env/support/LI-7700/topics/change-log.html
3901 2019-04-11 Bouldin Corn Gas Analyzer CH4 Calibration Bouldin Corn Gas Analyzer CH4 Calibration Location: Bouldin Corn
Last calibration: 2018-10-25
RSSI=87%, Optical RH=22%
Ambient P=101.5kPa, Tair=19.1C
Zero Air M4002 at 1600psi, AMP C03923 3.121 at 1600
CH4 Zero Offset: 0.024ppm
CH4 Span Offset: -0.007ppm
Notes: Windy
3761 2018-10-25 Bouldin Corn Gas Analyzer CH4 Calibration Bouldin Corn Gas Analyzer CH4 Calibration Location: Bouldin Corn
Last calibration: 2018-04-04
RSSI=91%, Optical RH=16%
Ambient P=101.5kPa, Tair=27.2C
Zero Air at 1925psi, AMP Air 3.121 at 1975
CH4 Zero Offset: .015ppm
CH4 Span Offset: -.013ppm
Notes: Gently breezy day
3385 2018-04-05 Lab none Installed Bouldin Corn Gas Analyzer CH4 Installed at BC to replace sn TG1-0211, which was brought back to the lab for calibration.
3380 2018-04-04 Lab none Calibration Lab none Calibration Location: Lab
Last calibration: 2017-03-23
RSSI=87%, Optical RH=7%
Ambient P=100.7kPa, Tair=22.6C
Zero Air at 100psi, LBL Air 1.9497 at 1700
CH4 Zero Offset: .01ppm
CH4 Span Offset: -.005ppm
Notes:
3197 2017-11-10 East End Gas Analyzer CH4 Removed Lab none Removed from EE and brought back to the lab for calibration. It was replaced by sn TG1-0357.
2672 2017-03-23 East End Gas Analyzer CH4 Calibration East End Gas Analyzer CH4 Calibration Location: East End
Last calibration: 2016-10-11
RSSI=90.5%, Optical RH=25%
Ambient P=102.2kPa, Tair=14.6C
Zero Air at 750psi, Ameriflux CH4 4.0304 at 850
CH4 Zero Offset: -0.008ppm
CH4 Span Offset: -0.0251ppm
Notes: Changed dessicant but did not flush out head with dry air.
2491 2016-10-11 East End Gas Analyzer CH4 Calibration East End Gas Analyzer CH4 Calibration Location: East End
Last calibration: 2016-04-13
RSSI=82%, Optical RH=21%
Ambient P=101.6kPa, Tair=21.1C
zero air at 800psi, AMP CH4 4.030 at 1400
CH4 Zero Offset: 0.020ppm
CH4 Span Offset: 0.010ppm
Notes: Breezy
2236 2016-04-13 East End Gas Analyzer CH4 Calibration East End Gas Analyzer CH4 Calibration Location: East End
Last calibration: 2015-09-30
RSSI=86.86%, Optical RH=12%
Ambient P=101.2kPa, Tair=20.94C
Zero Air at 950psi, AMP CH4 1.9966 at 850
CH4 Zero Offset: 0.002ppm
CH4 Span Offset: -0.010ppm
Notes: Gusty breeze
1947 2015-09-30 East End Gas Analyzer CH4 Calibration East End Gas Analyzer CH4 Calibration Location: East End
Last calibration: 2015-05-28
RSSI=73%, Optical RH=5%
Ambient P=101.5kPa, Tair=18.8C
Zero Air at 1000psi, AMP CH4 1.9966 at 1600
CH4 Zero Offset: 0.014ppm
CH4 Span Offset: 0.0024ppm
Notes: Raining, breezy, The clock was reading 1970 on arrival - fixed before calibration.
1858 2015-05-28 East End Gas Analyzer CH4 Calibration East End Gas Analyzer CH4 Calibration Location: East End
Last calibration: 2015-01-21
RSSI=84%, Optical RH=4%
Ambient P=101.54kPa, Tair=21C
Zero Air at 1200psi, AMP CH4 1.9966 at 2050
CH4 Zero Offset: 0.026ppm
CH4 Span Offset: 0.0ppm
Notes: Light breeze, partly cloudy, warm
1729 2015-02-05 Lab none Installed East End Gas Analyzer CH4 Installed on the East End tower to replace sn TG1-0224 that has the pump control problem
1688 2015-02-02 Factory Returned Lab none Returned from Licor on RMA 00186861 for internal corrosion due to a leak. Licor says: Replace corroded connector LED board. We couldn't see any way that the water got inside. Very strange. We did add some water resistant grease under the spinning mirror that is now a part of how we build all instruments. The analog board had some component that was shorting out all the 5 volts for the whole instrument causing the lights to blink and motor spin. replaced the board. calibrated instrument.
1689 2015-01-21 Factory Calibration Factory Calibration Location: Factory
Last calibration: 2014-09-10
RSSI=%, Optical RH=%
Ambient P=kPa, Tair=C
at psi, at
CH4 Zero Offset: ppm
CH4 Span Offset: ppm
Notes: Factory calibration by Licor on RMA 00186861. Zero = -28.6916, span = 9.94586e-05
1687 2015-01-08 Lab none Shipped Factory Sent to Licor on RMA 00186861. On power up the mirror would spin at top speed for a while then shut down with all three green LEDs blinking on the bottom. I found corrosion from water on the boards after opening the bottom can.
1686 2014-12-23 East End Gas Analyzer CH4 Removed Lab none On power up the mirror would spin at top speed and not stop. Removed for testing in the lab.
1546 2014-09-10 East End Gas Analyzer CH4 Calibration East End Gas Analyzer CH4 Calibration Location: East End
Last calibration: 2014-03-07
RSSI=80%, Optical RH=23%
Ambient P=101.23kPa, Tair=29.9C
Zero Air at 1400psi, 2nd CH4 4.995 at 700
CH4 Zero Offset: 0.085ppm
CH4 Span Offset: -0.195ppm
Notes: Very hot day with no wind. Offsets larger than usual.
1232 2014-03-07 East End Gas Analyzer CH4 Calibration East End Gas Analyzer CH4 Calibration Location: East End
Last calibration: 2013-03-20
RSSI=85%, Optical RH=19%
Ambient P=102.8kPa, Tair=16.3C
Zero Air at 1600psi, 2nd CH4 4.995 at 1100
CH4 Zero Offset: 0.03ppm
CH4 Span Offset: 0.015ppm
Notes: Calibrated by Cove and Sara. Firmware upgraded to v1.0.21 before cal. Windy day. A little fluctuation in span 5.01-4.995
1541 2014-02-25 Twitchell Alfalfa Gas Analyzer CH4 Installed East End Gas Analyzer CH4 Installed on the East End Tower with its wash box to replace sn TG1-0203 that was returned to Frank. This instrument came directly from Alfalfa.
1540 2014-02-25 Twitchell Alfalfa Gas Analyzer CH4 Removed East End Gas Analyzer CH4 Removed from the Alfalfa tower along with its wash box to be installed on the East End Tower to replace sn TG1-0203 that was returned to Frank
1069 2013-08-28 Lab none Installed Twitchell Alfalfa Gas Analyzer CH4 Installed on the Twitchell Alfalfa tower with washer box. Plugged in to the existing 7550 box.
955 2013-03-20 Lab none Calibration Lab none Calibration Location: Lab
Last calibration: 2012-10-31
RSSI=89%, Optical RH=4%
Ambient P=100.8kPa, Tair=23C
UHP N2 at 1100psi, 2nd CH4 in air 3.875 at 1800
CH4 Zero Offset: 0.0ppm
CH4 Span Offset: 0.035ppm
Notes: Last calibrated by Frank Anderson.
819 2012-10-25 Mayberry-Portable Loaned Loaned Removed from the Mayberry Portable Tower and loaned to Frank Anderson for use by the USGS on Statten Island in the Delta
837 2012-09-06 Mayberry-Portable Calibration Mayberry-Portable Calibration Location: Mayberry Portable
Last calibration: 2012-07-27
RSSI=72%, Optical RH=%
Ambient P=101.4kPa, Tair=16.3C
ultra zero air at 1900psi, ch4 in air 4.982 at 950
CH4 Zero Offset: 0.025ppm
CH4 Span Offset: 0.036ppm
Notes: Last calibration was by Licor after repair for misaligned spars. Calibrated on the portable tower by Joe and Cove.
716 2012-08-02 Lab none Installed Mayberry-Portable Installed on the Mayberry Portable tower. A loaner 7700 from Licor was removed to be returned to Licor.
685 2012-07-27 Factory Repair Lab none Returned from Licor. Under warrenty they replaced the spar and spar clamps. After repair it would lose signal strength under cold conditions. Replacing the spinning mirror assembly fixed this problem. It was fully calibrated:
Zero = -23.6232, span = 9.5816e-05, lasermoddepth = 17000, laserstarttemp = 21, blockstarttemp = 30, blockstarttemplowrange = 5, rssidropthresh = 0, pzero = 57.5, pspan = 15.27, samplegain = 0, refgain = 0, mirrorpos = 0, offset1 = 32000, delta1 = 0, offset2 = 0, delta2 = 0, dither = 30000, sampledcoffset = 443, sampleacoffset = -965, sampleopticaloffset = 0
620 2012-05-29 Lab none Shipped Factory Sent to Licor for repair on RMA 169766 - probably loose spars maybe covered by recall.
619 2012-05-25 Mayberry-Portable Removed Lab none Removed from portable tower at Mayberry. RSSI is about zero probably because loose spars allowed it to get misaligned.
731 2012-05-10 Lab none Installed Mayberry-Portable Installed with the Mayberry Portable tower in the back on the truck.
835 2012-04-27 Lab none Calibration Lab none Last calibration: 2011-01-19
RSSI=85%, Optical RH=3%
Ambient P=101.2kPa, Tair=23.8C
zero air at 300psi, ch4 in air 4.982 at 1800
CH4 Zero Offset: 0.024ppm
CH4 Span Offset: 0.099ppm
Notes: Calibrated in the the lab by Jaclyn
549 2012-04-24 Mayberry Gas Analyzer CH4 Removed Lab none Removed from the Mayberry eddy tower. Replaced with LI-7700 sn TG1-0224
505 2011-11-22 Mayberry Gas Analyzer CH4 Calibration Mayberry Gas Analyzer CH4 After cleaning the mirrors the RSSI was 69. We tried to check the calibration of the LI7700. I put the hood on the 7700 and ran zero air through it. I watched the value on the CR1000. It got down to about 10ppb - not as good as I expected. I tried to run a span gas but didn't have the correct regulator.
504 2011-06-30 Mayberry Gas Analyzer CH4 Calibration Mayberry Gas Analyzer CH4 I removed the solar shield and installed the calibration hood. I was able to connect to the LI7700 through the LI7550 using Ethernet. I changed the wash cycle from 20sec spray rechecked every 15min to a 10sec spray rechecked every 3hr as suggested by Liukang. I flowed zero air from a small transfer tank at about 400psi. The LI7700 reported 0ppm CH4. I then flowed 1.976ppm secondary standard from the tank that used to be at Sherman. The LI7700 reported 1.976ppm CH4. Because the LI7700 seemed to be right on I did not to a formal calibration.
503 2011-02-03 Lab none Installed Mayberry Gas Analyzer CH4 Installed on the Mayberry tower to replace the 7700 that was on loan to us from Licor. Collecting data on the CR1000 by direct ethernet to 7700.
284 2011-01-31 Lab none Calibration Lab none On 1/27/11, Dennis and Jaclyn tested the LI-7700 output against the calibration gases in the lab.

1. The tank with 4.982 ppm methane read 5.021 ppm on the LI-7700.
2. The zero air tank read 0.05 ppm on the LI-7700 (although low confidence that the gas is in fact zero methane.
3. The 1.8978 god bottle read 1.898 on the LI-7700.

We chose not to calibrate the instrument since the readings were so close to the actual values.
280 2011-01-25 Factory Returned Lab none Returned from repair at Licor. Service note say: "The spars were knocked out of alignment. The spinning mirror bearings were knocked out of alignment. Replaced the motor and realigned everything. Tested in environmental chamber from -25C to 50C. Calibrated.

Changes to settings:
Zero = 23.0176
Span = 0.00010261

sampledcoffset = 430
samplescoffset = -965
279 2010-12-22 Lab none Repair Factory The new LI-7700 was returned to Licor for repair.
278 2010-12-08 Lab none Initial settings Lab none Zero = -27.0097
Span = 0.00010248
lasermoddepth = 16850
laserstarttemp = 21.8
blockstrattemp = 30
blockstarttemplowrange = 5
rssidropthresh = 0
pzero = 57.5
pspan = 15.27
samplegain = 0
refgain = 0
mirrorpos = 0
offset1 = 31500
delta1 = 70
offset2 = 0
delta2 = 0
dither = 30000
sampledcoffset = 419
sampleacoffset = -960
sampleopticaloffset = 0

IPV6 = fe80:021c:94ff:fe04:04fe
IPV4 = 169.254.125.82