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Equipment and Calibration

View History

Equipment Entry

Instrument:Gas Analyzer
Manufacture:Los Gatos Research
Model No:FMA RMT-200
Serial No:05-0010
Tag No:20051000785
Acquisition Date:2005-12-16
Project:NSF-Methane
Location on 2020-02-25:Lab, NULL
Notes: NULL

Documents

Manual: LGR_FMA_DataSheet.pdf
Manual: LGR_RMT-FMA_UsersGuide07-C.pdf
Manual: LGR_FMA_MirrorCleaning.pdf
Manual: LGR_FMA_MirrorDisassembly.pdf

History

Rec No.DateLoc FromTitleLoc ToNotes
4396 2020-02-25 Lab Notes Lab We removed the pressure controller from this unit for use in the other LGR sn 08-0114. We did not reinstall a pressure controller.
2526 2014-05-20 Lab none Damaged Lab none After being moved, but not treated roughly, the analyzer stopped reporting CH4. The ring time is variable from 2 to 20usec and the spectrum looks odd. Cleaning the mirrors made no difference. LGR thinks there is something wrong with the laser. At this time there is an 8 week wait for repairs and a minimum cost of 00 for cleaning and calibration - any repairs would be an additional cost. We don't need this analyzer right now and will wait to repair it.
1819 2014-01-10 Sherman Island Removed Lab none Removed from the box at Sherman due to low pressure readings. Replaced by sn 08-0114
1026 2013-06-18 Lab none Installed Sherman Island Installed at Sherman by Cove to replace sn 08-0114 that was refusing to boot.
1005 2013-06-17 Lab none Calibration Lab none Last calibration: 2012-03-18
Cell Pressure=156.27Torr, Cell Temperature=24.76C, Ring Time=12.762usec
Primary CH4 in Air at >1900 psi
CH4 Span=1.89919 ppm
CH4 = 1.895 -> 1.899 Offset: -4ppb
Notes: Done in the lab with primary NOAA GMD standard. Cross cal with secondary CH4 tank = 4.995 ppm (n = 164). Placed new label on secondary CH4 tank. Last cross cal of 4.982 ppm on June 2, 2010.
946 2013-03-18 Lab none Calibration Lab none Last calibration: 2012-08-23
Cell Pressure=157.32Torr, Cell Temperature=24.40C, Ring Time=12.694usec
2nd CH4 in Air at psi
CH4 Span=3.875ppm
CH4 = 3.888 -> 3.872 Offset: -13ppb
Notes: Done in the lab after cleaning the 10um filter infront of the pressure controller
947 2013-03-14 Sherman Island Removed Lab none Removed from the Sherman Island box by Cove due to low pressure in the low flow mode. Replaced by sn 08-0114.
745 2012-08-23 Lab none Installed Sherman Island Installed in the box at Sherman by Cove. This is to replace sn 08-0114 that has had low pressure when running on the internal pump.
744 2012-08-23 Lab none Calibration Lab none Last calibration: 2012-05-01
Cell Pressure=156.91Torr, Cell Temperature=21.20C, Ring Time=13.885usec
CH4 in air at 1500psi
CH4 Span=4.982ppm
CH4 = 4.931 -> 4.988 Offset: 51ppb
Notes:
556 2012-04-24 Twitchell Rice Removed Lab none Removed from the box at Twitchell, replced with LI-7700
1495 2012-01-25 Twitchell Rice Calibration Twitchell Rice With the new external filter I calibrated the LGR. The cal tank has <200psi of 3.276ppm CH4. Last calibration was Dec 20, 2011.
Pre Cal: 8:49PST, 29.61C, 156.07Torr, 13.871usec, 3.282ppm, 1Hz

The first try at calibration failed somehow ending in a value (3.317ppm) farther from the span gas. A second calibration seemed to work fine and ended up right on.

When I left the LGR read
9:56PST, 23.93C, 153.81Torr, 13.060usec, 10Hz, 2.311ppm
1494 2011-12-18 Twitchell Rice Calibration Twitchell Rice All was running. The LGR read:
9:04PST, 31.36C, 97.41Torr, 13.973usec, 10Hz, 2.964ppm

I calibrated the LGR with secondary tank with 3.276ppm CH4 at 250psi. Last cal was 2011-11-22
Pre cal: 9:12PST, 30.18C, 124.54Torr, 13.972usec, 1Hz, 3.200ppm
Pressure was a little low but okay. After cal the LGR read 3.271ppm. I adjusted the bypass valve to bring the pressure to 146Torr in high flow mode. I returned the LGR to 10Hz before leaving.
1493 2011-11-22 Twitchell Rice Calibration Twitchell Rice We calibrated the LGR with a 3.276ppm tank with 400psi. Last cal was Oct 10, 2011.
9:56PST, 9.53C, 156.07Torr, 14.341usec, 1Hz, 3.357ppm
After cal it was right on. When we left it was back in high flow at 10Hz and pressure was about 141Torr, I did not adjust the bypass valve.
1492 2011-10-27 Lab none Installed Twitchell Rice Installed to replace sn 08-0114 since in slow flow mode there was zero flow.
422 2011-10-10 Lab none Calibration Lab none I calibrated the LRG with the god bottle and then used it to check two secondary standards. God bottel is 1.8978ppm CH4 and 350psi. Last calibration was 2011-08-23 using 3.276ppm CH4.
Precal: 9:32PST, 23.79C, 156.56Torr, 14.715usec, 1Hz, 1.855ppm
Postcal the CH4 read 1.897ppm.

The older secondary standard with 405.85ppm CO2 read 4.675ppm CH4
The newer secondary standard with 410.49ppm CO2 read 3.228ppm CH4
421 2011-10-10 Lab none Maintenance Lab none No flow in low flow mode. The internal 2um after the pressure controller seemed okay. I disassembled the inlet tubing and fittings to get a 10um filter out from infront of the pressure controller. This was completely plugged. I rinsed it with degreaser and DI water and dried it by blowing air through it. Flow was better but still seemed low. I reinstalled the filter and reassembled the inlet tubing. Now is slow flow the internal pressure is 156Torr.
401 2011-09-02 Loaned Returned Lab none This analyzer was returned by Frank after completion of their chamber campaign.
398 2011-08-22 Lab none Loaned Loaned Loaned to Frank for chamber campaign in Twitchell ponds during the week of August 22nd, 2011.
386 2011-08-16 Lab none Calibration Lab none See calibration log. I also set the time to local standard time and changed the serial settings to 115200. I left it in high flow and shutdown so it should boot correctly next time.
385 2011-08-12 Lab none Repair Lab none This analyzer was removed from the field because it would not boot. Connecting the hard drive to a computer running Knopix Linux I could see that the drive was full and deleted some of the data files. Then it would boot but the analyzer software would crash and kick out into the service shell. There I could see that a bunch of the *.ini files in the icos folder were zero length. LGR was able to email me a copy of these files and replacing them seemed to fix the problems.
374 2011-06-10 Twitchell Rice Removed Lab none Removed from Twitchell island because it was hanging up during boot. Frank discovered it on June 6th.
1488 2011-03-22 Twitchell Rice Calibration Twitchell Rice Pre cal: 8:42PST, 17.16C, 156.57Torr, 17.042usec, 1Hz, 3.347ppm � about 70ppb off.
Post cal: 3.277ppm

Before we left the LGR read:
8:55PST, 17.42C, 149.22Torr, 17.068usec, 10Hz, 2.176ppm
263 2011-01-18 Lab none Installed Twitchell Rice Installed to replace our other LGR FMA that suffered a power problem.
262 2010-11-29 Factory Returned Lab none Returned from factory repair. Replaced internal plumbing, throttle valve, solenoid valve, partical filter, laser driver board and cavity mirror. 41.72 total. Broken parts returned with analyzer.
261 2010-10-19 Lab none Repair Factory This FMA was sent to the factory for repair. RMA 10-0139
312 2010-10-01 Twitchell Rice Removed Lab none The air conditioning had failed or been over come by unusually hot weather and the box got really hot (~60C). The LGR had crashed but the pump was running. Starting at stopping the pump and LGR might have back flushed fine particals into the cell. The ring time was down to 4usec. I removed the LGR for mirror cleaning.
1489 2010-05-13 Twitchell Rice Calibration Twitchell Rice The LGR was reporting:
8:27PDT, 22.89C, 120.58Torr, 16.781usec, 10Hz, 1.858ppm

I adjusted the bypass valve to correct the pressure. I calibrated the LGR with 3.276ppm tank with 700psi. Last cal was March 22, 2011
Precal: 8:47PDT. 24.11C, 156.50Torr, 16.776usec, 1Hz, 3.290ppm
After cal 3.276ppm
Before I left the LGR read:
8:52PDT, 24.49C, 150.77Torr, 16.774usec, 10Hz, 1.883ppm
191 2010-04-21 Lab none Installed Sherman Island This analyzer is fresh from factory service. I installed it to replace sn 08-0114 suffering from low pressure.
99 2010-04-07 Factory Repair Lab none Returned from LGR. LGR bill says pressure controller, filter, and check valve were replaced. Mirrors were cleaned. Running in slow flow mode analyzer is reporting 156.20 Torr and 18.587 usec ring time.
73 2010-03-04 Sherman Island Removed Lab none This analyzer was removed from Sherman for maintenance - low pressure on internal pump. It is now in the lab.
310 2010-01-14 Sherman Island Calibration Sherman Island Calibrated with 1.976ppm CH4 secondary standard in the field. Pre-cal the LGR read 1.981ppm at 19.67C, 59.08Torr, 14.747usec.
309 2009-12-28 Sherman Island Calibration Sherman Island Calibration checked with 1.976ppm CH4 secondary standard in the field. LGR read 1.976ppm at 17.79C and 58.5Torr. No calibration necessary.
306 2009-11-19 Sherman Island Calibration Sherman Island Calibrated with 1.976ppm CH4 secondary standard in the field. Pre-cal LGR read 2.014ppm. Last calibration was 9-17-2009
82 2009-09-17 Lab none Installed Sherman Island Installed. Calibrated in field with 1.976ppm CH4 secondary standard. Pre-cal LGR read 1.933ppm at 19.58C, 156.38Torr, 18.178usec.
83 2009-08-12 Lab none Calibration Factory Calibrated with 1.898ppm CH4 source - possibly at factory.
162 2009-08-06 Sherman Island Removed Lab none Removed from the box at Sherman Island for mirror cleaning because the ring time was 10.8usec.
307 2009-07-09 Sherman Island Calibration Sherman Island Calibrated with 1.976ppm CH4 secondary standard in the field. Pre-cal LGR read 1.994ppm.
308 2009-06-09 Sherman Island Calibration Sherman Island Notes from 7-9-2010 say that the LGR reports its last calibration was June 9th.
206 2009-03-11 Sherman Island Removed Lab none Removed from the Sherman tower for mirror cleaning.
84 2009-03-08 Lab none Repair Factory Returned to factory for problem with pressure controller. Factory cleaned dirty pressure controller.
 
 

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