Equipment and Calibration

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Equipment Entry

Instrument:Gas Analyzer
Manufacture:Los Gatos Research
Model No:FGGA
Serial No:09-0010
Tag No:NULL
Acquisition Date:0000-00-00
Project:Borrowed
Location on 2014-04-22:Returned, NULL
Notes: NULL

Documents

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History

Rec No.DateLoc FromTitleLoc ToNotes
337 2011-03-21 Lab none Adjusted Lab none I had to adjust the line lock for CH4 and H2O again. I changed it from 0.245 to 0.255. Also some strange computer lock up pausing on boot. But seems okay.
219 2010-09-29 Moffett Field Removed Lab none Removed with portable tower from the zero flux study at Moffett Field.
212 2010-09-23 Lab none Installed Moffett Field This analyzer was installed with a portable tower at Moffett Field for a week long zero flux study.
201 2010-09-07 Lab none Maintenance Lab none This analyzer ran in the lab with no flow in slow flow mode and the cell pressure started close to 138Torr and fell slowly. I replaced the internal 2um filter with no improvement. A high flow of lab bench air through the filter before installing seems to have cleaned the down stream side of the filter and did not foul the mirrors.

I bought a new pressure controller from LGR ($720) and installed it. Cell pressure was 138Torr and holding steady with good flow.

I had to change the linelock v0 value from 0.215 to 0.225 to get CH4 and H2O to lock.
179 2010-08-17 Twitchell Rice Removed Lab none Removed from Twitchell for low to no flow in slow flow mode. Need to trouble shoot in the lab.
1485 2010-06-22 Twitchell Rice Calibration Twitchell Rice Initial readings from the LGR were:
9:57, 29.18C, 129.50Torr, 13.902usec, 10Hz, 1.865ppm, 14819ppm, 385.91ppm

I tried calibrating and notice very low pressure in low flow mode � 74.89Torr. I completed the calibration, but did not like it. I checked the exterior 2um filter and it seemed okay. I also checked the internal 2um filter and it seemed good as well. In checking the interior I noticed a loose connection. The connector that has to be disconnected to clean the mirror was left disconnected last time I cleaned the mirrors. I�m asking LGR what this connection does. It doesn�t look significant but after connecting it the pressure improved somewhat. And I did a second calibration.

Precal: last cal June 3, 3.276ppm CH4, 433.0ppm CO2, 1800psi
10:54, 134.32Torr, 3.217+-0.003ppm CH4, 416+-2ppm CO2

Post cal: 10:57, 130.0Torr, 3.276+-0.002ppm CH4, 433+-1ppm CO2

Last readings from LGR:
11:02, 28.57C, 144.47Torr, 13.86usec, 10Hz, 1.888ppm, 15195ppm, 400.44ppm
1484 2010-06-03 Twitchell Rice Calibration Twitchell Rice Calibrated with 3.276ppm CH4 and 433.0ppm CO2 tank 1750psi. Last cal May 20, 2010
Precal: 10:26, 129.6Torr dropping to 119Torr, 3.30+-0.05ppm CH4, 430+-1ppm CO2
Postcal: 3.26+-0.001ppm CH4, 429+-1ppm CO2

System back at 10Hz.
1483 2010-05-20 Twitchell Rice Calibration Twitchell Rice calibrated the LGR:

Initial readings:
9:35, 19.99C, 138.24Torr, 14.071usec, 10Hz, 1.8530ppm, 8187ppm, 406.97ppm

bypass valve adjusted to 143.55Torr. Calibrated with 3.276ppm CH4, 433.0ppm CO2 tank with 1800psi

Pre cal: 9:41, 138.16Torr, 1Hz, 3.220+-0.005ppm, 444+-1ppm
Post cal: 9:48, 3.278+-0.002ppm, 432+-1ppm

Ambient conditions after calibration:
9:50, 20.02C, 143.90Torr, 14.069usec, 10Hz, 1.8610ppm, 8332ppm, 390.55ppm
1482 2010-05-05 Twitchell Rice Calibration Twitchell Rice Twitchell: cal gas 3.276 ppm CH4, 433ppm CO2, mirror 13.9 us, 145 Torr, 37C
CH4 pre-cal: 3.342
CO2 pre-cal: 441
CH4 post-cal: 3.273
CO2 post-cal: 433
1481 2010-04-22 Twitchell Rice Calibration Twitchell Rice The LGR would not line lock CH4/H2O when power was restored. Initially the cell temperature was about 10C and I let it warm up to 18C with no lock and many restarts. Finally I called LGR and got their maintenance password to change line lock settings from 0.165 to 0.185 and this did the trick.

Initial readings
11:35, 18.50C, 144.60Torr, 13.940usec, 10Hz, 2.149ppm, 12039ppm, 398.07ppm

Calibrated with 3.276ppm CH4, 433.0ppm CO2 tank, last cal Mar 11, 2010
Precal 11:40, 138.24Torr, 3.270+-0.002ppm CH4, 425.0+-1ppm CO2
Postcal: 11:44, 138Torr, 3.279+-0.002ppm CH4, 433.5+-1ppm CO2
2142 2010-04-08 Twitchell Rice Calibration Twitchell Rice Last calibration: 2010-03-11
Cell Pressure=134.99Torr, Cell Temperature=26.64C, Ring Time=14.014usec
2nd Standard at 1900psi CH4 Span=3.276ppm, CO2 Span=433.0ppm
CH4 = 3.302 -> 3.305 Offset: -0.026ppm
CO2 = 436 -> 439 Offset: -3ppm
Notes: Seems to have made it worse?
71 2010-03-04 Lab none Installed Twitchell Rice This analyzer was installed at twitchell so that the other one could be removed for maintenance. This anaylzer had inital line lock problems, but has running properly when I left.
2141 2010-03-03 Lab none Calibration Lab none Last calibration: 2010-01-14
Cell Pressure=138.16Torr, Cell Temperature=20.17C, Ring Time=13.987usec
God CH4 at psi CH4 Span=1.8978ppm, CO2 Span=382.50ppm
CH4 = 1.834 -> 1.903 Offset: 0.064ppm
CO2 = 354 -> 383 Offset: 28.5ppm
Notes: Testing with CH4 standard 4.978ppm CH4 and 3ppm CO2 LGR reading: 4.785ppm +- 9ppb CH4 CO2 reading -1.00 Maybe out of range Testing with CO2 standard 597.4ppm CO2 ??ppm CH4 LGR reading: 2.701ppm +- 9ppb CH4 LGR reading: 582ppm +-4ppm CO2 This analyzer seems noisier than the single channel. Will check other FGGA analyzer after swap.
69 2010-03-03 Borrowed Initial Notes Lab none This analyzer was borrowed from Frank Anderson